Fast method for synthesis of alkyl and aryl-N-methylnitrones

Fast method for synthesis of alkyl and aryl-N-methylnitrones

A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by...

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Veröffentlicht in:Molecules (Basel, Switzerland) Switzerland), 2011-08, Vol.16 (8), p.6677-6683
Hauptverfasser: Yavuz, Serkan, Ozkan, Hamdi, Colak, Naki, Yildirir, Yilmaz
Format: Artikel
Sprache:eng
Schlagworte:
Chemistry, Organic - methods
grinding
Methods
Nitrogen Oxides - chemical synthesis
Nitrogen Oxides - chemistry
nitrone
Proton Magnetic Resonance Spectroscopy
solid-phase synthesis
solventless
Solvents
Time Factors
Transition Temperature
Vacuum distillation
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Beschreibung
Zusammenfassung:A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.
ISSN:1420-3049
1420-3049
DOI:10.3390/molecules16086677