A green chemical route for the synthesis of Mn3O4 nanoparticles

A novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn 3 O 4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmi...

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Veröffentlicht in:	Central European Journal of Chemistry 2009-09, Vol.7 (3), p.555-559
Hauptverfasser:	Durmus, Zehra, Kavas, Hüseyin, Baykal, Abdulhadi, Toprak, Muhammet S.
Format:	Artikel
Sprache:	eng
Schlagworte:	[BMIM]OH Biochemistry Biological and Medical Physics Biophysics Chemistry Chemistry and Materials Science Chemistry/Food Science EPR Geochemistry Ionic liquids Mn3O4 Nanoparticles Research Article TEM
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	A novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn 3 O 4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmission electron microscopy. Phase purity was confirmed by XRD, and X-ray line profile fitting determined a crystallite size of 42 ± 11 nm. TEM analysis revealed various morphologies. EPR measurements have indicated the existence of long-range interactions, due to the wide range of particle sizes and morphologies observed.
ISSN:	1895-1066 2391-5420 1644-3624 2391-5420
DOI:	10.2478/s11532-009-0049-4