5-(1H-Indol-3-yl)-1-methyl-3-phenyl-1,6-benzodiazocin-2(1H)-one

5-(1H-Indol-3-yl)-1-methyl-3-phenyl-1,6-benzodiazocin-2(1H)-one

The title compound, 5-(1H-indol-3-yl)-1-methyl-3-phenyl-1,6-benzodiazocin-2(1H)-one, was synthesized for the first time by a one-step, two-component reaction between 1-methylbenzimidazole and benzoylindolyl-3-acetylene. The product was characterized by 1H-NMR, 13C-NMR, IR spectroscopy and HRMS.

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Bibliographische Detailangaben
Veröffentlicht in:MolBank 2022-12, Vol.2022 (4), p.M1466
Hauptverfasser: Belyaeva, Kseniya V., Tomilin, Denis N., Afonin, Andrei V., Trofimov, Boris A.
Format: Artikel
Sprache:eng
Schlagworte:
Acetylene
Conflicts of interest
diazocinones
electron-deficient acetylenes
Infrared spectroscopy
nitrogen heterocycles
NMR
Nuclear magnetic resonance
ring-expansion
Spectrum analysis
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Zusammenfassung:The title compound, 5-(1H-indol-3-yl)-1-methyl-3-phenyl-1,6-benzodiazocin-2(1H)-one, was synthesized for the first time by a one-step, two-component reaction between 1-methylbenzimidazole and benzoylindolyl-3-acetylene. The product was characterized by 1H-NMR, 13C-NMR, IR spectroscopy and HRMS.
ISSN:1422-8599
1422-8599
DOI:10.3390/M1466