Preparation and electrochemical performance of nano-silver-graphene composite by electroless plating

Using glucose as the reducing agent, the nano-silver-graphene composite material (Ag/GR) was synthesized in situ by electroless plating, the structural morphology of the material was characterized and analyzed by X-ray diffraction (XRD), X-ray energy dispersive spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), scanning electron microscope (SEM) and Fourier infrared spectrometry (FTIR). The results show that the loading morphology of silver on the graphene surface is the single state that meets the expectation. The average particle size of AgNPs is about 21 nm. At the same time, the electrochemical response of ascorbic acid (AA) on Ag/GR/GCE electrochemical sensors was studied using the electrochemical test methods of cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), linear sweep voltammetry (LSV) and differential pulse voltammetry (DPV). The electrochemical test results show that the Ag/GR composite has the highest response electrochemical signal of 212.9 μA and the lowest resis