Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid

Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid

  5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which  have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I).       Their charact...

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Veröffentlicht in:Ibn Al-Haitham Journal for Pure and Applied Sciences 2017-04, Vol.26 (1)
Hauptverfasser: Muhanned J. Mahmoud, Redha I. AL-bayati, Shaimaa A. Saoud, Ismaeel Y. Majeed
Format: Artikel
Sprache:eng
Schlagworte:
1,3,4-thiadiazole derivative
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Zusammenfassung:  5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which  have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I).       Their characterization was carried out from T.L.C, M.P, FT.IR and 1H-NMR.
ISSN:1609-4042
2521-3407