1-(4-Carboxybutan-2-ylidene)-4-phenylthiosemicarbazide
The molecule of the title compound, C 12 H 15 N 3 O 2 S, which belongs to the family of thiosemicarbazones, containing an acid group, adopts a semi-closed conformation with an intramolecular N—H...N hydrogen bond. In the crystal, molecules are linked by strong N—H...O and O—H...S hydrogen bonds betw...
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| Veröffentlicht in: | Acta crystallographica. Section E, Structure reports online Structure reports online, 2012-06, Vol.68 (6), p.o1945-o1946 |
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| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | The molecule of the title compound, C
12
H
15
N
3
O
2
S, which belongs to the family of thiosemicarbazones, containing an acid group, adopts a semi-closed conformation with an intramolecular N—H...N hydrogen bond. In the crystal, molecules are linked by strong N—H...O and O—H...S hydrogen bonds between the acid group and thiosemicarbazone unit, with one additional intermolecular hydrogen C—H...O interaction. These three interactions form
R
2
2
(8) and a
R
2
1
(7) rings and the molecules related by the
c
-glide plane are linked into a zigzag chain along [001]. |
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| ISSN: | 1600-5368 1600-5368 |
| DOI: | 10.1107/S1600536812023793 |