Entada Gigas seeds mediated synthesis of carbon for dielectric and sensing applications

In the current work, a plant-based carbon sample is synthesized successfully from monkey ladder (EntadaGigas) plant seeds by combustion technique. The prepared samples are subjected to characterizations such as Powder X-ray Diffractogram(PXRD), Scanning Electron Microscopy (SEM), Fourier Transform I...

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Veröffentlicht in:Sensors international 2022, Vol.3, p.100162, Article 100162
Hauptverfasser: Sudheer Kumar, K.H., Yashaswini, Yashwanth, H.J., Pratibha, S., Hareesh, K., Manohara, S.R.
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Sprache:eng
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Zusammenfassung:In the current work, a plant-based carbon sample is synthesized successfully from monkey ladder (EntadaGigas) plant seeds by combustion technique. The prepared samples are subjected to characterizations such as Powder X-ray Diffractogram(PXRD), Scanning Electron Microscopy (SEM), Fourier Transform Infrared Spectroscopy (FTIR), Energy Dispersive X-ray (EDX) Analysis. The PXRD pattern of the prepared MLC carbon sample exhibits the graphitic structure. The SEM micrograph displays the flake-like morphology; the FTIR spectrum reveals the presence of carbon-based functional groups. The dielectric property of the prepared carbon sample has been studied and confirms the good ac conductivity. The cole-cole plot of the prepared MLC carbon sample displays a single semicircle which signifies the highly resistive grain boundaries. The electrochemical study of prepared MLC Coated Ni foam electrode in 0.1 ​M NaOH electrolyte solution showed good redox potential output proposed by cyclic voltammetric and amperometric studies.The developed material exhibited a good response towards the glucose sensor with a sensitivity of 0.8 mAmM-1 and a limit of detection of 0.5 ​mM. •MLC based carbon sample was synthesized successfully by simple combustion method.•The dielectric study confirms that the prepared sample is a promising candidate for high frequency applications.•The synthesized carbon sample exhibits good glucose sensing.
ISSN:2666-3511
2666-3511
DOI:10.1016/j.sintl.2022.100162