Electron crystallography with the EIGER detector

Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a...

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Veröffentlicht in:IUCrJ 2018-03, Vol.5 (Pt 2), p.190-199
Hauptverfasser: Tinti, Gemma, Fröjdh, Erik, van Genderen, Eric, Gruene, Tim, Schmitt, Bernd, de Winter, D A Matthijs, Weckhuysen, Bert M, Abrahams, Jan Pieter
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Sprache:eng
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Zusammenfassung:Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 × 75 µm , frame rates up to 23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data.
ISSN:2052-2525
2052-2525
DOI:10.1107/S2052252518000945