Electron crystallography with the EIGER detector
Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a...
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Veröffentlicht in: | IUCrJ 2018-03, Vol.5 (Pt 2), p.190-199 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Electron crystallography is a discipline that currently attracts much attention as method for inorganic, organic and macromolecular structure solution. EIGER, a direct-detection hybrid pixel detector developed at the Paul Scherrer Institut, Switzerland, has been tested for electron diffraction in a transmission electron microscope. EIGER features a pixel pitch of 75 × 75 µm
, frame rates up to 23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation transfer functions of the detector at 100, 200 and 300 keV electron energies are reported and the data quality is demonstrated by structure determination of a SAPO-34 zeotype from electron diffraction data. |
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ISSN: | 2052-2525 2052-2525 |
DOI: | 10.1107/S2052252518000945 |