An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst

The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Veröffentlicht in:	Bulletin of chemical reaction engineering & catalysis 2018-12, Vol.13 (3), p.436-446
Hauptverfasser:	Magar, Rameshwar R., Pawar, Ganesh T., Gadekar, Sachin P., Lande, Machhindra Karbhari
Format:	Artikel
Sprache:	eng
Schlagworte:	1,8-dioxo-octahydroxanthene 5,5-dimethyl-cyclohexane-1,3-dione aromatic aldehyde Catalysis Catalysts ce-zsm-11 zeolite Chemical synthesis Cyclohexane Derivatives Diketones Fourier transforms Infrared analysis Scanning electron microscopy Spectrum analysis X ray powder diffraction X ray spectra X-ray diffraction Zeolites
Online-Zugang:	Volltext
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), Fourier Transform Infrared Spectroscopy (FTIR), Brunauer-Emmer-Teller (BET) surface area analysis, and Temperature Programmed Desorption (TPD) techniques. This method provides several advantageous such as use of inexpensive catalyst, simple work-up procedure, high yield of desired product and reusability of catalyst.
ISSN:	1978-2993 1978-2993
DOI:	10.9767/bcrec.13.3.2062.436-446