Surface Morphology of Silica Films Derived by the Sol-Gel Method and Its Application to a Water Repellent Glass

Silica films with various surface morphologies, such as flatness, mesoporosity, uneveness, convexity, were prepared by hydrolysis and polymerization of tetraethoxysilane, Si(OC2H5)4(TEOS) and methyltrietoxysilane, CH3Si(OC2H5)3(MTES) under acid-catalyzed conditions. The morphology of coatings could...

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Veröffentlicht in:Journal of the Ceramic Society of Japan 1997/11/01, Vol.105(1227), pp.1012-1017
Hauptverfasser: MAKITA, Kensuke, AKAMATSU, Yoshinori, YAMAZAKI, Seiji, KAI, Yasuaki, ABE, Yoshihiro
Format: Artikel
Sprache:eng ; jpn
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Zusammenfassung:Silica films with various surface morphologies, such as flatness, mesoporosity, uneveness, convexity, were prepared by hydrolysis and polymerization of tetraethoxysilane, Si(OC2H5)4(TEOS) and methyltrietoxysilane, CH3Si(OC2H5)3(MTES) under acid-catalyzed conditions. The morphology of coatings could be changed by changing the molar ratio (denoted as f, f=KITES/TEOS) in TEOS-MTES mixture, as well as the conditions of drying process and heat treatment temperature. Especially, in the case of 5
ISSN:0914-5400
1882-1022
DOI:10.2109/jcersj.105.1012