SiO2:MgMnO3: An Efficient Heterogeneous Catalyst for One Pot Synthesis of 1H-Pyrazolo[1,2-b]phthalazine-5,10-dione Derivatives
The present study deals with hydrothermal synthesis of SiO2 composite MgMnO3 catalyst. The obtained polycrystalline product was analyzed by using physical investigative techniques including XRD, SEM, EDAX, TEM, SAED and BET surface area. The product corresponded to average particle size of 100 nm by...
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Veröffentlicht in: | Asian journal of chemistry 2020-10, Vol.32 (10), p.2489-2494 |
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Hauptverfasser: | , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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Zusammenfassung: | The present study deals with hydrothermal synthesis of SiO2 composite MgMnO3 catalyst. The obtained
polycrystalline product was analyzed by using physical investigative techniques including XRD, SEM,
EDAX, TEM, SAED and BET surface area. The product corresponded to average particle size of 100
nm by TEM images. The BET surface area was found 234.38 cm2/g for SiO2 composite MgMnO3
catalyst which indicates a good catalytic property. The synthesized catalyst was applied for the synthesis
of 1H-pyrazolo[1,2-b]-phthalazine-5,10-dione in presence of ethanol as a solvent at 80 ºC. The current
procedure and catalyst offers the gains of clean reaction, short reaction time, high yield, easy purification
and financial availability of the catalyst. |
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ISSN: | 0970-7077 0975-427X |
DOI: | 10.14233/ajchem.2020.22707 |