Reversed Phase-Behaviour of 16,17-Secoestrone Derivatives in LC

The chromatographic behaviour of a number of 16,17-secoestrone derivatives, has been studied by LC on non-polar chemically bonded stationary phases C-8 and C-18 commercially available columns. The mobile phases used were: methanol-water and acetonitrile-water in various proportions. The separation a...

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Veröffentlicht in:	Chromatographia 2010, Vol.71 (9-10), p.913-916
Hauptverfasser:	Ačanski, Marijana M, Dobrijević, Jelena P, Redžepović, Azra S, Vujić, Đura N, Sakač, Marija M, Jovanović-Šanta, Suzana S
Format:	Artikel
Sprache:	eng
Schlagworte:	16,17-Secoestrone derivatives Analytical Chemistry Chemistry Chemistry and Materials Science Chromatographic methods and physical methods associated with chromatography Chromatography Column liquid chromatography Correlation analysis Exact sciences and technology Full Short Communication Laboratory Medicine Other chromatographic methods Pharmacy Proteomics
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	The chromatographic behaviour of a number of 16,17-secoestrone derivatives, has been studied by LC on non-polar chemically bonded stationary phases C-8 and C-18 commercially available columns. The mobile phases used were: methanol-water and acetonitrile-water in various proportions. The separation ability is discussed in terms of nature of the solute, eluent, and stationary phase. The correlation between the retention constants of 16,17-secoestrone derivatives with log P calculated by using commercial program ACD log P software has also been examined.
ISSN:	0009-5893 1612-1112
DOI:	10.1365/s10337-010-1537-6