A SHORT STEP AND PRACTICAL SYNTHESIS OF MYO-INOSITOL 1, 3, 4, 5-TETRAKISPHOSPHATE
The reaction of myo-inositol with benzoly chloride gave 1, 3, 4, 5-tetra-O-benzoyl-myo-inositol as a major product which was conveniently converted to myo-inositol 1, 3, 4, 5-tetrakisphosphate. The tetrabenzoate was optically resolved by means of chiral column chromatography using Chiralcel OD.
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| Veröffentlicht in: | Chemical & pharmaceutical bulletin 1990/02/25, Vol.38(2), pp.562-563 |
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| container_end_page | 563 |
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| container_issue | 2 |
| container_start_page | 562 |
| container_title | Chemical & pharmaceutical bulletin |
| container_volume | 38 |
| creator | WATANABE, Yutaka SHINOHARA, Tomoiti FUJIMOTO, Takahiro OZAKI, Shoichiro |
| description | The reaction of myo-inositol with benzoly chloride gave 1, 3, 4, 5-tetra-O-benzoyl-myo-inositol as a major product which was conveniently converted to myo-inositol 1, 3, 4, 5-tetrakisphosphate. The tetrabenzoate was optically resolved by means of chiral column chromatography using Chiralcel OD. |
| doi_str_mv | 10.1248/cpb.38.562 |
| format | Article |
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Pharm. Bull.</addtitle><description>The reaction of myo-inositol with benzoly chloride gave 1, 3, 4, 5-tetra-O-benzoyl-myo-inositol as a major product which was conveniently converted to myo-inositol 1, 3, 4, 5-tetrakisphosphate. The tetrabenzoate was optically resolved by means of chiral column chromatography using Chiralcel OD.</description><subject>benzoylation</subject><subject>Carbohydrates with 4, 5, 6, ... C atoms, dissacharides and oligosaccharides</subject><subject>Carbohydrates. Nucleosides and nucleotides</subject><subject>Chemistry</subject><subject>chiral column chromatography</subject><subject>Exact sciences and technology</subject><subject>myo-inositol</subject><subject>myo-inositol 1, 3, 4, 5-tetrakisphosphate</subject><subject>Organic chemistry</subject><subject>phosphorylation</subject><subject>Preparations and properties</subject><issn>0009-2363</issn><issn>1347-5223</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1990</creationdate><recordtype>article</recordtype><recordid>eNpFkLFOwzAQhi0EEqWw8AReWFBTbJ_tJGMUUhJRmtKYoVPkODa0KlDFXXh7UgXR4e6G_7tv-BG6pWRKGY8ezL6ZQjQVkp2hEQUeBoIxOEcjQkgcMJBwia683xLCBAlhhF4TXOXlSuFKZUucLB7xcpWkqkiTOa7WC5VnVVHhcoZf1mVQLMqqUOUc0wmGCeYTLAKVqVXyXFTLvOwnUdk1unB65-3N3x2jt1mm0jyYl09HbWC4lCygAiLttCRgNTDOjWxb2zgjRNPaGHqIszg0DTDHItLEQrbc0obE3FknnIQxuh-8pvv2vrOu3nebT9391JTUxzLqvowaorovo4fvBnivvdE71-kvs_Gnj5iJUFDouXTgtv6g3-0_oLvDxuzsUUljER21bFi9_ZR-6K62X_ALe7tu6Q</recordid><startdate>1990</startdate><enddate>1990</enddate><creator>WATANABE, Yutaka</creator><creator>SHINOHARA, Tomoiti</creator><creator>FUJIMOTO, Takahiro</creator><creator>OZAKI, Shoichiro</creator><general>The Pharmaceutical Society of Japan</general><general>Maruzen</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>1990</creationdate><title>A SHORT STEP AND PRACTICAL SYNTHESIS OF MYO-INOSITOL 1, 3, 4, 5-TETRAKISPHOSPHATE</title><author>WATANABE, Yutaka ; SHINOHARA, Tomoiti ; FUJIMOTO, Takahiro ; OZAKI, Shoichiro</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4662-1538afa603ea3244c6ddebfc55bde93c464297cb32f280b956d4e1b094fef5f63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1990</creationdate><topic>benzoylation</topic><topic>Carbohydrates with 4, 5, 6, ... C atoms, dissacharides and oligosaccharides</topic><topic>Carbohydrates. Nucleosides and nucleotides</topic><topic>Chemistry</topic><topic>chiral column chromatography</topic><topic>Exact sciences and technology</topic><topic>myo-inositol</topic><topic>myo-inositol 1, 3, 4, 5-tetrakisphosphate</topic><topic>Organic chemistry</topic><topic>phosphorylation</topic><topic>Preparations and properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>WATANABE, Yutaka</creatorcontrib><creatorcontrib>SHINOHARA, Tomoiti</creatorcontrib><creatorcontrib>FUJIMOTO, Takahiro</creatorcontrib><creatorcontrib>OZAKI, Shoichiro</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Chemical & pharmaceutical bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>WATANABE, Yutaka</au><au>SHINOHARA, Tomoiti</au><au>FUJIMOTO, Takahiro</au><au>OZAKI, Shoichiro</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A SHORT STEP AND PRACTICAL SYNTHESIS OF MYO-INOSITOL 1, 3, 4, 5-TETRAKISPHOSPHATE</atitle><jtitle>Chemical & pharmaceutical bulletin</jtitle><addtitle>Chem. Pharm. Bull.</addtitle><date>1990</date><risdate>1990</risdate><volume>38</volume><issue>2</issue><spage>562</spage><epage>563</epage><pages>562-563</pages><issn>0009-2363</issn><eissn>1347-5223</eissn><coden>CPBTAL</coden><abstract>The reaction of myo-inositol with benzoly chloride gave 1, 3, 4, 5-tetra-O-benzoyl-myo-inositol as a major product which was conveniently converted to myo-inositol 1, 3, 4, 5-tetrakisphosphate. The tetrabenzoate was optically resolved by means of chiral column chromatography using Chiralcel OD.</abstract><cop>Tokyo</cop><pub>The Pharmaceutical Society of Japan</pub><doi>10.1248/cpb.38.562</doi><tpages>2</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | Chemical and Pharmaceutical Bulletin, 1990/02/25, Vol.38(2), pp.562-563 |
| issn | 0009-2363 1347-5223 |
| language | eng |
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| source | J-STAGE Free; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Free Full-Text Journals in Chemistry |
| subjects | benzoylation Carbohydrates with 4, 5, 6, ... C atoms, dissacharides and oligosaccharides Carbohydrates. Nucleosides and nucleotides Chemistry chiral column chromatography Exact sciences and technology myo-inositol myo-inositol 1, 3, 4, 5-tetrakisphosphate Organic chemistry phosphorylation Preparations and properties |
| title | A SHORT STEP AND PRACTICAL SYNTHESIS OF MYO-INOSITOL 1, 3, 4, 5-TETRAKISPHOSPHATE |
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