Crystallizing Process of Amorphous Thick Films of Ferroelectric Lead Germanate Family

Real-time investigation of crystallizing processes of amorphous thick films of ferroelectric lead germanate (PGO) and silicon-doped PGO (PGSO) is carried out using a high-temperature X-ray diffraction system. Two irreversible phase transitions took place near 370° C and 530° C on heating: the first...

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Veröffentlicht in:Japanese Journal of Applied Physics 1994, Vol.33 (9S), p.5521
Hauptverfasser: Jun Hatano, Jun Hatano, Tomonori Mukaigawa, Tomonori Mukaigawa, Hiroyuki Uehara, Hiroyuki Uehara, Alexei Gruverman, Alexei Gruverman, Koichiro Takahashi, Koichiro Takahashi, Ken Yukino, Ken Yukino
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container_issue 9S
container_start_page 5521
container_title Japanese Journal of Applied Physics
container_volume 33
creator Jun Hatano, Jun Hatano
Tomonori Mukaigawa, Tomonori Mukaigawa
Hiroyuki Uehara, Hiroyuki Uehara
Alexei Gruverman, Alexei Gruverman
Koichiro Takahashi, Koichiro Takahashi
Ken Yukino, Ken Yukino
description Real-time investigation of crystallizing processes of amorphous thick films of ferroelectric lead germanate (PGO) and silicon-doped PGO (PGSO) is carried out using a high-temperature X-ray diffraction system. Two irreversible phase transitions took place near 370° C and 530° C on heating: the first is the crystallization from the amorphous to a metastable crystal state, and the second is from the metastable to a ferroelectric stable state of Pb 5 Ge 3 O 11 . Both transitions were completed very quickly, i.e., within approximately 7 and 58 min, respectively. The optimum heat-treatment conditions for fabricating well-oriented polycrystalline films were discussed together with the results of quick heating and quenching experiments.
doi_str_mv 10.1143/JJAP.33.5521
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title Crystallizing Process of Amorphous Thick Films of Ferroelectric Lead Germanate Family
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