Hydrothermal preparation of magnetite from iron chelates

The hydrothermal decomposition of iron(II) or iron(III) aminopolycarboxylate complexes can produce well-crystallized, stoichiometric Fe 3 O 4 . Best results were obtained when 0.1 m nitrilotriacetatoiron(III) was decomposed under N 2 in 0.2-0.4 m NaOH at 497 K for 70 h or more.

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Veröffentlicht in:Canadian journal of chemistry 1978-02, Vol.56 (3), p.402-403
Hauptverfasser: Booy, Meindert, Swaddle, Thomas Wilson
Format: Artikel
Sprache:eng
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Zusammenfassung:The hydrothermal decomposition of iron(II) or iron(III) aminopolycarboxylate complexes can produce well-crystallized, stoichiometric Fe 3 O 4 . Best results were obtained when 0.1 m nitrilotriacetatoiron(III) was decomposed under N 2 in 0.2-0.4 m NaOH at 497 K for 70 h or more.
ISSN:0008-4042
1480-3291
DOI:10.1139/v78-064