Photolysis and mass spectra of trans-cinnamimide
Using Pyrex filtered light, irradiation of trans-cinnamimide in 1,2-dimethoxyethane solution gave β-truxinimide (48% yield), cis-cinnamamide and trans-cinnamamide. Both trans-cinnamimide and β-truxinimide undergo fragmentation in the mass spectrometer to give C 16 H 14 +, C 16 H 13 +, C 16 H 12 +...
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| Veröffentlicht in: | Canadian journal of chemistry 1969-09, Vol.47 (17), p.3250-3254 |
|---|---|
| Hauptverfasser: | , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | Using Pyrex filtered light, irradiation of trans-cinnamimide in 1,2-dimethoxyethane solution gave β-truxinimide (48% yield), cis-cinnamamide and trans-cinnamamide. Both trans-cinnamimide and β-truxinimide undergo fragmentation in the mass spectrometer to give C
16
H
14
+, C
16
H
13
+, C
16
H
12
+, and C
14
H
12
+. |
|---|---|
| ISSN: | 0008-4042 1480-3291 |
| DOI: | 10.1139/v69-534 |