The composition of commercial acetylated glycerol samples determined by 13C and 1H NMR. The comparison with gas chromatography
A convenient method for the analysis of commercial acetylated glycerol samples based on 13 C NMR is presented with the accuracy comparable to the standard gas chromatography approaches. The advantage of method is that it does not need any sample derivatization procedure by silyl groups and its appli...
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| Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2014-08, Vol.69 (8), p.763-768 |
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| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | A convenient method for the analysis of commercial acetylated glycerol samples based on
13
C NMR is presented with the accuracy comparable to the standard gas chromatography approaches. The advantage of method is that it does not need any sample derivatization procedure by silyl groups and its application is much more straightforward, as compared to the published
1
H NMR method. |
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| ISSN: | 1061-9348 1608-3199 |
| DOI: | 10.1134/S1061934814080103 |