Template assisted synthesis of CaO-SnO2 nanocomposites
Calcium oxide (CaO) and tin oxide (SnO 2 ) with nanodimension have attracted significant attention as effective chemosorbents for toxic compounds. Hydrothermal method was used for the synthesis of highly porous CaO-SnO 2 nanocomposites by using sodium dodecylsulfate surfactant as a templating agent....
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Veröffentlicht in: | Russian Journal of Physical Chemistry A 2015-06, Vol.89 (6), p.1051-1058 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Calcium oxide (CaO) and tin oxide (SnO
2
) with nanodimension have attracted significant attention as effective chemosorbents for toxic compounds. Hydrothermal method was used for the synthesis of highly porous CaO-SnO
2
nanocomposites by using sodium dodecylsulfate surfactant as a templating agent. Effect of concentration of surfactant as well as its critical micelle concentration (CMC) on the particle size of the nanocomposites was investigated. X-ray diffraction (XRD) was used to determine the crystal phases of these nanocomposites and particle size and morphology was identified by using transmission electron microscopy (TEM), scanning electron microscopy-energy dispersive X-ray (SEM/EDX) respectively. Furthermore thermo gravimetric analysis (TGA) and fourier transform infrared (FTIR) spectroscopy techniques were also used to characterize the CaO-SnO
2
nanocomposites. |
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ISSN: | 0036-0244 1531-863X |
DOI: | 10.1134/S0036024415060059 |