New versions of circular thin-layer chromatography on plates with a closed sorption layer

New versions of circular thin-layer chromatography (corner TLC and lateral TLC) with a closed sorption layer are proposed, studied, and compared with traditional methods of linear and circular TLC. The use of a closed sorption layer in the new versions of circular chromatography is demonstrated to r...

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Veröffentlicht in:Russian Journal of Physical Chemistry A 2010-11, Vol.84 (11), p.1962-1966
Hauptverfasser: Berezkin, V. G., Chausov, A. V.
Format: Artikel
Sprache:eng
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Zusammenfassung:New versions of circular thin-layer chromatography (corner TLC and lateral TLC) with a closed sorption layer are proposed, studied, and compared with traditional methods of linear and circular TLC. The use of a closed sorption layer in the new versions of circular chromatography is demonstrated to reduce the duration of separation (by 15–20%) while lowering the efficiency of separation negligibly. The feasibility of TLC with a closed sorption layer is demonstrated for the determination of highly volatile compounds.
ISSN:0036-0244
1531-863X
DOI:10.1134/S0036024410110245