New versions of circular thin-layer chromatography on plates with a closed sorption layer
New versions of circular thin-layer chromatography (corner TLC and lateral TLC) with a closed sorption layer are proposed, studied, and compared with traditional methods of linear and circular TLC. The use of a closed sorption layer in the new versions of circular chromatography is demonstrated to r...
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Veröffentlicht in: | Russian Journal of Physical Chemistry A 2010-11, Vol.84 (11), p.1962-1966 |
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Hauptverfasser: | , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | New versions of circular thin-layer chromatography (corner TLC and lateral TLC) with a closed sorption layer are proposed, studied, and compared with traditional methods of linear and circular TLC. The use of a closed sorption layer in the new versions of circular chromatography is demonstrated to reduce the duration of separation (by 15–20%) while lowering the efficiency of separation negligibly. The feasibility of TLC with a closed sorption layer is demonstrated for the determination of highly volatile compounds. |
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ISSN: | 0036-0244 1531-863X |
DOI: | 10.1134/S0036024410110245 |