SYNTHESIS, CHARACTERIZATION, AND COMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA- 1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE

SYNTHESIS, CHARACTERIZATION, AND COMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA- 1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE

N -[(9E)-8,10,17-Triazatetracyclo[8.7.0.0 2,7 .0 11,16 ]heptadeca-1(17),2,4,6,11(16),12,14-heptaen-9-ylidene] benzamide ( I ) is synthesized and characterized by spectroscopy, microanalysis, and single crystal X-ray diffractometry. Compound I crystallizes in the monoclinic space group P 2 1 / c with...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Journal of structural chemistry 2020-08, Vol.61 (8), p.1177-1185
Hauptverfasser: Odame, F., Hosten, E. C., Tshentu, Z. R.
Format: Artikel
Sprache:eng
Schlagworte:
Atomic
Atomic/Molecular Structure and Spectra
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Molecular
Optical and Plasma Physics
Physical Chemistry
Solid State Physics
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:N -[(9E)-8,10,17-Triazatetracyclo[8.7.0.0 2,7 .0 11,16 ]heptadeca-1(17),2,4,6,11(16),12,14-heptaen-9-ylidene] benzamide ( I ) is synthesized and characterized by spectroscopy, microanalysis, and single crystal X-ray diffractometry. Compound I crystallizes in the monoclinic space group P 2 1 / c with a  = 15.8980(7) Å, b  = 4.8067(2) Å, c  = 21.0455(10) Å, β = 101.153(2)°, and Z  = 4. The experimental bond lengths and bond angles are contrasted with computed bond lengths and bond angles.
ISSN:0022-4766
1573-8779
DOI:10.1134/S0022476620080016