Synthesis and Structural Characterization of Benzene-1,3-disulfonamide-containing 11- to 13-membered Heterocycles via Double Mitsunobu Annulation

Synthesis and Structural Characterization of Benzene-1,3-disulfonamide-containing 11- to 13-membered Heterocycles via Double Mitsunobu Annulation

The synthesis and conformation of several novel benzene-1,3-disulfonamides-containing 11- to 13-membered heterocycles have been achieved. Double Mitsunobu annulation was effective for construction of medium to large ring systems in moderate chemical yields. In addition, the flexibility of sulfonamid...

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Veröffentlicht in:Chemistry letters 2024-01
Hauptverfasser: Kaneda, Kyosuke, Koideya, Takato, Toshima, Ryuji, Konno, Yoshiki, Yamagishi, Takehiro
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container_title Chemistry letters
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creator Kaneda, Kyosuke
Koideya, Takato
Toshima, Ryuji
Konno, Yoshiki
Yamagishi, Takehiro
description The synthesis and conformation of several novel benzene-1,3-disulfonamides-containing 11- to 13-membered heterocycles have been achieved. Double Mitsunobu annulation was effective for construction of medium to large ring systems in moderate chemical yields. In addition, the flexibility of sulfonamide moieties in these rings was determined by X-ray crystal structural analysis.
doi_str_mv 10.1093/chemle/upad016
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title Synthesis and Structural Characterization of Benzene-1,3-disulfonamide-containing 11- to 13-membered Heterocycles via Double Mitsunobu Annulation
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