Green synthesis of Bryophyllum pinnatum aqueous leaf extract mediated bio-molecule capped dilute ferromagnetic α-MnO 2 nanoparticles

Bio-molecule capped α -MnO 2 nanoparticles have been successfully synthesized from the reduction of KMnO 4 via a facile green synthesis route using an aqueous leaf extract of Bryophyllum pinnatum as a reducing and capping agent. The synthesized α -MnO 2 nanoparticles were characterized by x-ray diff...

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Veröffentlicht in:Materials research express 2020-01, Vol.7 (1), p.15088
Hauptverfasser: Ullah, A K M Atique, Haque, Md Mahbubul, Akter, Mahmuda, Hossain, A, Tamanna, A N, Hosen, Md Mottaleb, Kibria, A K M Fazle, Khan, M N I, Khan, M K A
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Sprache:eng
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Zusammenfassung:Bio-molecule capped α -MnO 2 nanoparticles have been successfully synthesized from the reduction of KMnO 4 via a facile green synthesis route using an aqueous leaf extract of Bryophyllum pinnatum as a reducing and capping agent. The synthesized α -MnO 2 nanoparticles were characterized by x-ray diffraction (XRD), Fourier transform—infrared (FT-IR), energy dispersive x-ray (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), thermogravimetric (TG) and differential scanning calorimetry (DSC) techniques. Experimental results clearly demonstrate the successful synthesis of bio-molecule capped crystalline tetragonal α -MnO 2 nanoparticles with the size of 4–18 nm. The magnetic property of the product was evaluated using a vibrating sample magnetometer (VSM) and the result reveals that the presently synthesized bio-molecule capped α -MnO 2 nanoparticles exhibit ferromagnetic property at room temperature.
ISSN:2053-1591
2053-1591
DOI:10.1088/2053-1591/ab6c20