ONE-POT AND SIMPLE REACTION FOR THE SYNTHESIS OF ALKYL p-TOLUENESULFINATE ESTERS UNDER SOLID-PHASE CONDITIONS

ONE-POT AND SIMPLE REACTION FOR THE SYNTHESIS OF ALKYL p-TOLUENESULFINATE ESTERS UNDER SOLID-PHASE CONDITIONS

A manipulatively one-pot and rapid method for the synthesis of alkyl p-toluenesulfinate esters 1 from p-toluenesulfinic acid, supported thionyl chloride on silica gel and aliphatic alcohols in solid phase conditions is described.

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Bibliographische Detailangaben
Veröffentlicht in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2000-05, Vol.160 (1), p.67-75
Hauptverfasser: Hajipour, A. M., Mallakpour, S. E., Afrousheh, A.
Format: Artikel
Sprache:eng
Schlagworte:
Chiral synthesis
p-Toluenesulfinic acid
Silica gel
Solid-phase conditions
Sulfinate esters
Thionyl chloride
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Beschreibung
Zusammenfassung:A manipulatively one-pot and rapid method for the synthesis of alkyl p-toluenesulfinate esters 1 from p-toluenesulfinic acid, supported thionyl chloride on silica gel and aliphatic alcohols in solid phase conditions is described.
ISSN:1042-6507
1563-5325
DOI:10.1080/10426500008043672