Solid-Liquid Phase Transfer Catalytic Synthesis X: The Rapid Alkylation of Ethyl Acetoacetate Under Microwave Irradiation

Solid-Liquid Phase Transfer Catalytic Synthesis X: The Rapid Alkylation of Ethyl Acetoacetate Under Microwave Irradiation

Rapid alkylation of ethyl acetoacetate with a series of halides were performed in 650W domestic microwave oven and the isolated yield of monoalkylated product varying from 59 to 82%.

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Veröffentlicht in:Synthetic communications 1994-01, Vol.24 (1), p.111-115
Hauptverfasser: Deng, Runhua, Wang, Yuliang, Jiang, Yaozhong
Format: Artikel
Sprache:eng
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Zusammenfassung:Rapid alkylation of ethyl acetoacetate with a series of halides were performed in 650W domestic microwave oven and the isolated yield of monoalkylated product varying from 59 to 82%.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397919408012633