Chemical shift scaling in NMR of rotating solids

Chemical shift scaling in NMR of rotating solids

An improved version of the chemical shift scaling multipulse cycle is demonstrated that eliminates the dependence of the direction of the axis of precession on the extent of scaling. This prevents the formation of a zero-frequency artifact in the final spectrum. Results from liquid, as well as stati...

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Veröffentlicht in:The Journal of chemical physics 1981-01, Vol.75 (12), p.5594-5595
Hauptverfasser: DiVerdi, J. A., Opella, S. J.
Format: Artikel
Sprache:eng
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Zusammenfassung:An improved version of the chemical shift scaling multipulse cycle is demonstrated that eliminates the dependence of the direction of the axis of precession on the extent of scaling. This prevents the formation of a zero-frequency artifact in the final spectrum. Results from liquid, as well as stationary and spinning solid samples, are described.
ISSN:0021-9606
1089-7690
DOI:10.1063/1.441996