Strain and Ge concentration determinations in SiGe/Si multiple quantum wells by transmission electron microscopy methods

SiGe/Si multiple quantum wells, nominally 4 nm thick, were grown by low pressure chemical vapor deposition and the Ge distribution within the wells was studied using a variety of transmission electron microscope-based techniques. Energy-dispersive x-ray spectroscopy and electron energy-loss imaging...

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Veröffentlicht in:Journal of applied physics 2003-04, Vol.93 (7), p.3893-3899
Hauptverfasser: Benedetti, A., Norris, D. J., Hetherington, C. J. D., Cullis, A. G., Robbins, D. J., Wallis, D. J.
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Sprache:eng
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Zusammenfassung:SiGe/Si multiple quantum wells, nominally 4 nm thick, were grown by low pressure chemical vapor deposition and the Ge distribution within the wells was studied using a variety of transmission electron microscope-based techniques. Energy-dispersive x-ray spectroscopy and electron energy-loss imaging were used to directly measure the Ge compositional profile across the SiGe wells. In addition, the average Ge concentration was deduced indirectly from measurement of the strain-induced lattice displacements in high resolution images, obtained from the relative phase shift of the Si lattice planes on either side of a SiGe well. The results from both the direct and indirect measurement techniques were compared and found to be in good agreement with one another. The Ge profiles exhibited an asymmetric shape consistent with the occurrence of Ge segregation during growth. However, the amplitude of the asymmetry indicated that an additional factor, in particular gas dwell times within the reactor, also needed to be taken into account. Based upon this approach, a successful theoretical model of the growth process was derived.
ISSN:0021-8979
1089-7550
DOI:10.1063/1.1558993