Deprotection of o-Nitrobenzensulfonyl (Nosyl) Derivatives of Amines ­Mediated by a Solid-Supported Thiol

Deprotection of o-Nitrobenzensulfonyl (Nosyl) Derivatives of Amines ­Mediated by a Solid-Supported Thiol

Abstract A new protocol based on a solid-supported thiol was ­developed for high yielding deprotection of O-nitrobenzensulfonyl amides derived from primary and secondary amines. The reaction can be carried out at room temperature for 24 hours or accelerated by microwave irradiation, going to complet...

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Veröffentlicht in:Synlett 2005-12, Vol.2005 (19), p.2996-2998
Hauptverfasser: Cardullo, Francesca, Donati, Daniele, Merlo, Giancarlo, Paio, Alfredo, Salaris, Margherita, Taddei, Maurizio
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container_end_page 2998
container_issue 19
container_start_page 2996
container_title Synlett
container_volume 2005
creator Cardullo, Francesca
Donati, Daniele
Merlo, Giancarlo
Paio, Alfredo
Salaris, Margherita
Taddei, Maurizio
description Abstract A new protocol based on a solid-supported thiol was ­developed for high yielding deprotection of O-nitrobenzensulfonyl amides derived from primary and secondary amines. The reaction can be carried out at room temperature for 24 hours or accelerated by microwave irradiation, going to completion in six minutes.
doi_str_mv 10.1055/s-2005-921892
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title Deprotection of o-Nitrobenzensulfonyl (Nosyl) Derivatives of Amines ­Mediated by a Solid-Supported Thiol
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