Preparation of (2-Methyl-propane-2-sulfonylimino) Acetic Acid Ethyl Ester

Preparation of (2-Methyl-propane-2-sulfonylimino) Acetic Acid Ethyl Ester

Abstract Synthesis of (2-methyl-propane-2-sulfonylimino) acetic acid ethyl ester from TERT-butylsulfonamide, thionyl chloride and ethyl glyoxylate is described. The N-TERT-butylsulfonyl imino ester has served as a substitute of the corresponding N-toluenesulfonyl imino ester in allylation reactions.

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Veröffentlicht in:Synthesis (Stuttgart) 2004-04, Vol.2004 (6), p.967-969
Hauptverfasser: Schleusner, Marcel, Koep, Stefan, Günter, Markus, Tiwari, Shashi K., Gais, Hans-Joachim
Format: Artikel
Sprache:eng
Schlagworte:
practical synthetic procedures
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Zusammenfassung:Abstract Synthesis of (2-methyl-propane-2-sulfonylimino) acetic acid ethyl ester from TERT-butylsulfonamide, thionyl chloride and ethyl glyoxylate is described. The N-TERT-butylsulfonyl imino ester has served as a substitute of the corresponding N-toluenesulfonyl imino ester in allylation reactions.
ISSN:0039-7881
1437-210X
DOI:10.1055/s-2004-815925