Trichloroisocyanuric Acid/NaNO2 as a Novel Heterogeneous System for the N-Nitrosation of N,N-Dialkylamines Under Mild Conditions

Trichloroisocyanuric Acid/NaNO2 as a Novel Heterogeneous System for the N-Nitrosation of N,N-Dialkylamines Under Mild Conditions

Abstract A combination of trichloroisocyanuric acid and sodium nitrite in the presence of wet SiO 2 was used as an effective nitrosating agent for the nitrosation of N,N-dialkyl amines to their corresponding nitroso derivatives under mild and heterogeneous conditions in moderate to excellent yields.

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Veröffentlicht in:Synlett 2002, Vol.2002 (6), p.1002-1004
Hauptverfasser: Zolfigol, Mohammad Ali, Choghamarani, Arash Ghorbani, Hazarkhani, Hassan
Format: Artikel
Sprache:eng
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Zusammenfassung:Abstract A combination of trichloroisocyanuric acid and sodium nitrite in the presence of wet SiO 2 was used as an effective nitrosating agent for the nitrosation of N,N-dialkyl amines to their corresponding nitroso derivatives under mild and heterogeneous conditions in moderate to excellent yields.
ISSN:0936-5214
1437-2096
DOI:10.1055/s-2002-31897