Preparation and Analysis of Bicyclic Polystyrene

Bicyclic polystyrene was prepared by combining atom transfer radical polymerization and click chemistry. The bicyclic polymer was separated from concurrently produced acyclic (branched) polymers through fractional precipitation, and its purity was quantified by two-dimensional liquid chromatography...

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Veröffentlicht in:	Macromolecules 2014-06, Vol.47 (12), p.3791-3796
Hauptverfasser:	Jeong, Jonghwa, Kim, Kihyun, Lee, Rooda, Lee, Sookyeong, Kim, Hyewon, Jung, Haeji, Kadir, Mohammad Abdul, Jang, Yujin, Jeon, Heung Bae, Matyjaszewski, Krzysztof, Chang, Taihyun, Paik, Hyun-jong
Format:	Artikel
Sprache:	eng
Schlagworte:	Applied sciences Exact sciences and technology Organic polymers Physicochemistry of polymers Polymerization Preparation, kinetics, thermodynamics, mechanism and catalysts
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	Bicyclic polystyrene was prepared by combining atom transfer radical polymerization and click chemistry. The bicyclic polymer was separated from concurrently produced acyclic (branched) polymers through fractional precipitation, and its purity was quantified by two-dimensional liquid chromatography analysis. The structure of bicyclic polymer was characterized by SEC, MALDI–TOF MS, 1H NMR, and FT-IR.
ISSN:	0024-9297 1520-5835
DOI:	10.1021/ma500391z