Efficient Synthesis of Polyhydroxylated Fullerene Derivatives via Hydrolysis of Polycyclosulfated Precursors

Cyclosulfated fullerene derivatives were hydrolyzed in the presence of water or in aqueous NaOH solution giving polyhydroxylated fullerenes. Both sulfated precursors and hydroxylated products were characterized. 7 figs.

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Bibliographische Detailangaben
Veröffentlicht in:	Journal of Organic Chemistry 1994-07, Vol.59 (14), p.3960-3968
Hauptverfasser:	Chiang, Long Y, Wang, Lee-Yih, Swirczewski, John W, Soled, Stuart, Cameron, Steve
Format:	Artikel
Sprache:	eng
Schlagworte:	40 CHEMISTRY ALCOHOLS Alicyclic compounds Alicyclic compounds, terpenoids, prostaglandins, steroids CHEMICAL PREPARATION CHEMICAL REACTION YIELD Chemistry Exact sciences and technology FULLERENES Organic chemistry OXIDATION PHOTOELECTRON SPECTROSCOPY Preparations and properties RADICALS REACTION INTERMEDIATES THERMAL GRAVIMETRIC ANALYSIS
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Beschreibung
Zusammenfassung:	Cyclosulfated fullerene derivatives were hydrolyzed in the presence of water or in aqueous NaOH solution giving polyhydroxylated fullerenes. Both sulfated precursors and hydroxylated products were characterized. 7 figs.
ISSN:	0022-3263 1520-6904
DOI:	10.1021/jo00093a030