Baeyer-Villiger Oxidation of Indan-1-ones: Monitoring of the Reaction by VPC and IR Spectroscopy
Indan-1-Ones are oxidized into dihydrocoumarins either by CF3CO3H, which is prepared from TFAA and 30% commercial H2O2 or by MCPBA in refluxing dichloroethane. VPC and IR analysis are used for monitoring of the reaction.
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| Veröffentlicht in: | Journal of chemical education 1995-12, Vol.72 (12), p.1142 |
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| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | Indan-1-Ones are oxidized into dihydrocoumarins either by CF3CO3H, which is prepared from TFAA and 30% commercial H2O2 or by MCPBA in refluxing dichloroethane. VPC and IR analysis are used for monitoring of the reaction. |
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| ISSN: | 0021-9584 1938-1328 |
| DOI: | 10.1021/ed072p1142 |