CuI Crystal Growth in Acetonitrile Solvent by the Cycle-Evaporation Method
Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra,...
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| Veröffentlicht in: | Crystal growth & design 2009-09, Vol.9 (9), p.3825-3827 |
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| container_issue | 9 |
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| container_title | Crystal growth & design |
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| creator | Pan, Jianguo Yang, Shuying Li, Yuebao Han, Lei Li, Xing Cui, Yuejie |
| description | Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra, and XRD were used to investigate the redox processes in the solution. The crystal was characterized by X-ray powder diffraction and differential thermal /thermogravimetry analysis. |
| doi_str_mv | 10.1021/cg900775a |
| format | Article |
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The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra, and XRD were used to investigate the redox processes in the solution. The crystal was characterized by X-ray powder diffraction and differential thermal /thermogravimetry analysis.</description><identifier>ISSN: 1528-7483</identifier><identifier>EISSN: 1528-7505</identifier><identifier>DOI: 10.1021/cg900775a</identifier><language>eng</language><publisher>Washington,DC: American Chemical Society</publisher><subject>Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Materials science ; Methods of crystal growth; physics of crystal growth ; Physics ; Theory and models of crystal growth; physics of crystal growth, crystal morphology and orientation</subject><ispartof>Crystal growth & design, 2009-09, Vol.9 (9), p.3825-3827</ispartof><rights>Copyright © 2009 American Chemical Society</rights><rights>2009 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a355t-c21591012de7f9ff1c39ddc5e0b3ad2926bc3a29509c9ce12b7632336a6038d53</citedby><cites>FETCH-LOGICAL-a355t-c21591012de7f9ff1c39ddc5e0b3ad2926bc3a29509c9ce12b7632336a6038d53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/cg900775a$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/cg900775a$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2763,27074,27922,27923,56736,56786</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22069621$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Pan, Jianguo</creatorcontrib><creatorcontrib>Yang, Shuying</creatorcontrib><creatorcontrib>Li, Yuebao</creatorcontrib><creatorcontrib>Han, Lei</creatorcontrib><creatorcontrib>Li, Xing</creatorcontrib><creatorcontrib>Cui, Yuejie</creatorcontrib><title>CuI Crystal Growth in Acetonitrile Solvent by the Cycle-Evaporation Method</title><title>Crystal growth & design</title><addtitle>Cryst. 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Growth Des</addtitle><date>2009-09-02</date><risdate>2009</risdate><volume>9</volume><issue>9</issue><spage>3825</spage><epage>3827</epage><pages>3825-3827</pages><issn>1528-7483</issn><eissn>1528-7505</eissn><abstract>Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra, and XRD were used to investigate the redox processes in the solution. The crystal was characterized by X-ray powder diffraction and differential thermal /thermogravimetry analysis.</abstract><cop>Washington,DC</cop><pub>American Chemical Society</pub><doi>10.1021/cg900775a</doi><tpages>3</tpages></addata></record> |
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| language | eng |
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| source | ACS Publications |
| subjects | Cross-disciplinary physics: materials science rheology Exact sciences and technology Materials science Methods of crystal growth physics of crystal growth Physics Theory and models of crystal growth physics of crystal growth, crystal morphology and orientation |
| title | CuI Crystal Growth in Acetonitrile Solvent by the Cycle-Evaporation Method |
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