CuI Crystal Growth in Acetonitrile Solvent by the Cycle-Evaporation Method

Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra,...

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Veröffentlicht in:	Crystal growth & design 2009-09, Vol.9 (9), p.3825-3827
Hauptverfasser:	Pan, Jianguo, Yang, Shuying, Li, Yuebao, Han, Lei, Li, Xing, Cui, Yuejie
Format:	Artikel
Sprache:	eng
Schlagworte:	Cross-disciplinary physics: materials science rheology Exact sciences and technology Materials science Methods of crystal growth physics of crystal growth Physics Theory and models of crystal growth physics of crystal growth, crystal morphology and orientation
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra, and XRD were used to investigate the redox processes in the solution. The crystal was characterized by X-ray powder diffraction and differential thermal /thermogravimetry analysis.
ISSN:	1528-7483 1528-7505
DOI:	10.1021/cg900775a