Internal Gas–Liquid Separation in Industrial Ebullated Bed Hydroprocessors
Ebullated bed reactors used in heavy oil upgrading internally recycle up to 90% of net liquid flow to maintain fluidized conditions. Internal phase separators result in significant gas re-entrainment within the recycled liquid, leading to high gas holdup (40 to 60%), reduced processing capacity, and...
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Veröffentlicht in: | Industrial & engineering chemistry research 2019-10, Vol.58 (40), p.18675-18683 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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Zusammenfassung: | Ebullated bed reactors used in heavy oil upgrading internally recycle up to 90% of net liquid flow to maintain fluidized conditions. Internal phase separators result in significant gas re-entrainment within the recycled liquid, leading to high gas holdup (40 to 60%), reduced processing capacity, and over-cracking of vapor products. Phase separation in two commercial designs is assessed using computational fluid dynamics and compared to pilot-scale results. Liquid short-circuiting within first-generation recycle pan designs was identified as a key factor, leading to a reduced separation efficiency of 1 to 2 mm bubbles compared to second-generation flow-through designs. Negligible performance improvements were observed for |
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ISSN: | 0888-5885 1520-5045 |
DOI: | 10.1021/acs.iecr.9b02201 |