Internal Gas–Liquid Separation in Industrial Ebullated Bed Hydroprocessors

Ebullated bed reactors used in heavy oil upgrading internally recycle up to 90% of net liquid flow to maintain fluidized conditions. Internal phase separators result in significant gas re-entrainment within the recycled liquid, leading to high gas holdup (40 to 60%), reduced processing capacity, and...

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Veröffentlicht in:Industrial & engineering chemistry research 2019-10, Vol.58 (40), p.18675-18683
Hauptverfasser: Lane, Chris D, Macchi, Arturo, McKnight, Craig A, Wiens, Jason, Donaldson, Adam A
Format: Artikel
Sprache:eng
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Zusammenfassung:Ebullated bed reactors used in heavy oil upgrading internally recycle up to 90% of net liquid flow to maintain fluidized conditions. Internal phase separators result in significant gas re-entrainment within the recycled liquid, leading to high gas holdup (40 to 60%), reduced processing capacity, and over-cracking of vapor products. Phase separation in two commercial designs is assessed using computational fluid dynamics and compared to pilot-scale results. Liquid short-circuiting within first-generation recycle pan designs was identified as a key factor, leading to a reduced separation efficiency of 1 to 2 mm bubbles compared to second-generation flow-through designs. Negligible performance improvements were observed for
ISSN:0888-5885
1520-5045
DOI:10.1021/acs.iecr.9b02201