Nondestructive determination of boron and cadmium in environmental materials by thermal neutron-prompt .gamma.-ray spectrometry

Prompt ..gamma.. rays from thermal neutron induced nuclear reactions have been used to measure trace quantities of B and Cd in industrial and standard materials. The technique provides a rapid nondestructive analysis for > 0.05 ..mu..g of B. Repetitive analyses show the method to have a precision...

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Veröffentlicht in:Anal. Chem.; (United States) 1976-12, Vol.48 (14), p.2139-2142
Hauptverfasser: Gladney, Ernest S, Jurney, Edward T, Curtis, David B
Format: Artikel
Sprache:eng
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Zusammenfassung:Prompt ..gamma.. rays from thermal neutron induced nuclear reactions have been used to measure trace quantities of B and Cd in industrial and standard materials. The technique provides a rapid nondestructive analysis for > 0.05 ..mu..g of B. Repetitive analyses show the method to have a precision of 5%. The presence of large quantities of Na degrades the accuracy and precision of the B analysis. The technique also provides a method for the determination of Cd although it is not sufficiently sensitive to provide a practical alternative to more conventional methods.
ISSN:0003-2700
1520-6882
DOI:10.1021/ac50008a021