Effect of Pt-Al coating on low-cycle fatigue behavior in a Ni-based single crystal superalloy at 760 °C

The effect of Pt-Al coating on low-cycle fatigue behavior of Ni-based single crystal superalloy at 760 °C was evaluated. The results show that Pt-Al coating does not change the cyclic stress response behavior of the Ni-based single crystal superalloy at 760 °C. Under the total strain amplitude from 0.6 % to 1.2 %, the cyclic stress amplitude value of Pt-Al coating samples is slightly lower than uncoated samples during cyclic deformation at the stable stage under the same applied total strain amplitude, and the fatigue life of Pt-Al coating samples is lower than uncoated ones, with an average fatigue life reduction of about 19.9 %. By the relation curve of comparing the cyclic strain amplitude with the reversals to failure, it is observed that the fatigue ductility coefficient ε′f of the Pt-Al coating sample is higher than the uncoated sample, the fatigue ductility index c and fatigue strength coefficient σ′f are lower than the uncoated sample, but the fatigue strength index b has little difference. It is found that the cyclic strength coefficient K′ and the cyclic strain hardening index n' of the Pt-Al coating sample are lower than the uncoated sample after fitting the curves of the relationship between cyclic stress amplitude and total strain amplitude. In addition, the cyclic stress amplitude of Pt-Al coating sample is slightly lower than uncoated sample under the same applied total strain amplitude. It was found by SEM that the cracks of both uncoated and Pt-Al coating samples initialized near the surface of the samples under low-cycle fatigue loading at 760 °C, and multiple crack sources began to spread into the substrate. It was found by TEM observation that at low strain amplitude (Δεt/2 = 0.6 %), the dislocations in both uncoated and Pt-Al coating samples mainly converged in γ, and a large number of dislocation debris gathered in the γ and dislocation entanglement was generated, while a small number of dislocations were observed to cut into γ'. The γ′ is seriously deformed and slightly rafted at Δεt/2 = 1.2 %, and a few dislocations are also observed in γ'.