Unveiling the recrystallization mechanism and kinetics parameters in cold-rolled dual-phase stainless steel using differential scanning calorimetry
The present work aims to assess the Recrystallization mechanism and Kinetics parameters in Cold-Rolled Dual-Phase stainless steel. For this purpose, Differential Scanning Calorimetry was used over a range of 5–20 K/mn of heating rate, to identify the classical kinetic parameters such as recrystalliz...
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Veröffentlicht in: | Journal of the Indian Chemical Society 2024-09, Vol.101 (9), p.101224, Article 101224 |
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Sprache: | eng |
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Zusammenfassung: | The present work aims to assess the Recrystallization mechanism and Kinetics parameters in Cold-Rolled Dual-Phase stainless steel. For this purpose, Differential Scanning Calorimetry was used over a range of 5–20 K/mn of heating rate, to identify the classical kinetic parameters such as recrystallization temperature, activation energy, and growth mechanism following 90 % reduction in thickness. The findings revealed that the recrystallization temperature increased with rising heating rates within the range [706.8–732] for the ferrite phase, as well as [1282.0–1360.3] K for the austenite phase. The estimated activation energies for ferrite and austenite recrystallization fell within the range of [207.2 ± 1.4–220.1 ± 2.5] kJ/mol and [220.2 ± 2.0–241.1 ± 4.0] kJ/mol, respectively. The Avrami parameter approached half-unity for both ferrite and austenite recrystallized phases for which results can be interpreted to be chiefly responsible for a general mechanism involving the growth of new grains with appreciable initial volume through a diffusion-controlled process.
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•The peak temperature of recrystallization of ferrite phase was from 706 to 732 K.•The peak temperature of recrystallization of austenite phase was from 1282 to 1360 K.•The activation energy was in the range of 207–220 kJ/mol for the ferrite phase.•The activation energy was in the range of 220–241 kJ/mol for the austenite phase.•The Avrami exponent was close to half-unity for both ferrite and austenite phases. |
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ISSN: | 0019-4522 |
DOI: | 10.1016/j.jics.2024.101224 |