Solvent-free synthesis of polysubstituted pyrroles catalyzed by ZnO nanorods

Solvent-free synthesis of polysubstituted pyrroles catalyzed by ZnO nanorods

An efficient zinc oxide nanorod-catalyzed one-pot strategy has been developed for the synthesis of polysubstituted pyrroles in very good yields. The present approach provides a three-component reaction between primary alkylamines, dialkyl acetylenedicarboxylates, and 2-chloro-1,3-dicarbonyl compound...

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Veröffentlicht in:Journal of the Iranian Chemical Society 2015-12, Vol.12 (12), p.2199-2204
Hauptverfasser: Sabbaghan, Maryam, Sanaeishoar, Haleh, Ghalaei, Azam, Sofalgar, Pegah
Format: Artikel
Sprache:eng
Schlagworte:
Analytical Chemistry
Biochemistry
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Organic Chemistry
Original Paper
Physical Chemistry
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Zusammenfassung:An efficient zinc oxide nanorod-catalyzed one-pot strategy has been developed for the synthesis of polysubstituted pyrroles in very good yields. The present approach provides a three-component reaction between primary alkylamines, dialkyl acetylenedicarboxylates, and 2-chloro-1,3-dicarbonyl compounds with several advantages such as short reaction time, high yields, solvent free, and little catalyst loading. After reaction course, ZnO nanorods can be recycled and reused without any apparent loss of activity which makes this process cost effective and hence eco-friendly. Graphical abstract
ISSN:1735-207X
1735-2428
DOI:10.1007/s13738-015-0697-6