Synthesis, crystal structure and thermal analysis of a new stilbazolium salt crystal

A new organic crystal of 4-N, N-dimethylamino-4＇-N＇-methyl-stilbazolium benzene sulfonate （DASBS） was synthesized and characterized for the first time. It is a derivative of 4-N, N-dimethylamino-4＇-N＇-methyl-stilbazolium tosylate （DAST） with the benzene sulfonate replacing p-toluenesulfonate. Single...

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Veröffentlicht in:	Frontiers of materials science 2015-06, Vol.9 (2), p.147-150
Hauptverfasser:	TENG, Bing, KONG, Weijin, FENG, Ke, YOU, Fei, CAO, Lifeng, ZHONG, Degao, HAO, Lun, SUN, Qing, SMAALEN, Sander van, GONG, Wenhui
Format:	Artikel
Sprache:	eng
Schlagworte:	Chemistry and Materials Science crystal growth DAST Materials Science organic crystal Research Article single crystal X-ray diffraction thermal analysis 合成晶体结构有机晶体热分析烷基苯磺酸钠甲苯磺酸酯芪盐
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Beschreibung
Zusammenfassung:	A new organic crystal of 4-N, N-dimethylamino-4＇-N＇-methyl-stilbazolium benzene sulfonate （DASBS） was synthesized and characterized for the first time. It is a derivative of 4-N, N-dimethylamino-4＇-N＇-methyl-stilbazolium tosylate （DAST） with the benzene sulfonate replacing p-toluenesulfonate. Single crystal XRD demonstrated that the crystal structure of DASBS. H20 was triclinic. The thermal analysis of this new crystal was also conducted, and the melting point was obtained to be 232℃.
ISSN:	2095-025X 2095-0268
DOI:	10.1007/s11706-015-0284-x