Effect of Curcuma longa tuber powder extract on size of silver nanoparticles prepared by green method
Biosynthesis of noble metal nanoparticles is a vast developing area of research. In the present study, silver nanoparticles (Ag-NPs) were synthesized from aqueous silver nitrate through a simple and biosynthetic route using water extract of Curcuma longa ( C. longa ) tuber powder, which acted simult...
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Veröffentlicht in: | Research on chemical intermediates 2014-03, Vol.40 (3), p.1313-1325 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Biosynthesis of noble metal nanoparticles is a vast developing area of research. In the present study, silver nanoparticles (Ag-NPs) were synthesized from aqueous silver nitrate through a simple and biosynthetic route using water extract of
Curcuma longa
(
C. longa
) tuber powder, which acted simultaneousl as a reductant and stabilizery. The as-prepared samples are characterized using UV–Visible, XRD, TEM, SEM, EDXF, and FT-IR techniques. The formation of Ag-NPs is evidenced by the appearance of the signatory brown color of the solution and UV–vis spectra. Formation of Ag/
C. longa
was determined by UV–Vis spectroscopy where surface plasmon absorption maxima can be observed at 457–415 nm from the UV–Vis spectrum. The XRD analysis shows that the Ag-NPs are of a face-centered cubic structure. Well-dispersed Ag-NPs with anisotropic and isotropic morphology for 5, 10, and 20 mL of
C. longa
water extract having a size less than 10 nm are seen in TEM images. The optimum volume extraction to synthesize smallest particle size was 20 mL with mean diameter and standard division 4.90 ± 1.42 nm. FT-IR spectrum indicates the presence of different functional groups in capping the nanoparticles with
C. longa
. The zeta potential analysis results indicated that the charge of
C. longa
was negative and increased in Ag/
C. longa
emulsion with increasing of volumes of extract used (10–20 mL). The most needed outcome of this work will be the development of value-added products from
C. longa
for biomedical and nanotechnology-based industries. |
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ISSN: | 0922-6168 1568-5675 |
DOI: | 10.1007/s11164-013-1040-4 |