Effect of Curcuma longa tuber powder extract on size of silver nanoparticles prepared by green method

Biosynthesis of noble metal nanoparticles is a vast developing area of research. In the present study, silver nanoparticles (Ag-NPs) were synthesized from aqueous silver nitrate through a simple and biosynthetic route using water extract of Curcuma longa ( C. longa ) tuber powder, which acted simult...

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Veröffentlicht in:Research on chemical intermediates 2014-03, Vol.40 (3), p.1313-1325
Hauptverfasser: Shameli, Kamyar, Ahmad, Mansor Bin, Shabanzadeh, Parvaneh, Jaffar Al-Mulla, Emad A., Zamanian, Ali, Abdollahi, Yadollah, Jazayeri, Seyed Davoud, Eili, Mahboobeh, Jalilian, Farid Azizi, Haroun, Rafiuz Zaman
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Sprache:eng
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Zusammenfassung:Biosynthesis of noble metal nanoparticles is a vast developing area of research. In the present study, silver nanoparticles (Ag-NPs) were synthesized from aqueous silver nitrate through a simple and biosynthetic route using water extract of Curcuma longa ( C. longa ) tuber powder, which acted simultaneousl as a reductant and stabilizery. The as-prepared samples are characterized using UV–Visible, XRD, TEM, SEM, EDXF, and FT-IR techniques. The formation of Ag-NPs is evidenced by the appearance of the signatory brown color of the solution and UV–vis spectra. Formation of Ag/ C. longa was determined by UV–Vis spectroscopy where surface plasmon absorption maxima can be observed at 457–415 nm from the UV–Vis spectrum. The XRD analysis shows that the Ag-NPs are of a face-centered cubic structure. Well-dispersed Ag-NPs with anisotropic and isotropic morphology for 5, 10, and 20 mL of C. longa water extract having a size less than 10 nm are seen in TEM images. The optimum volume extraction to synthesize smallest particle size was 20 mL with mean diameter and standard division 4.90 ± 1.42 nm. FT-IR spectrum indicates the presence of different functional groups in capping the nanoparticles with C. longa . The zeta potential analysis results indicated that the charge of C. longa was negative and increased in Ag/ C. longa emulsion with increasing of volumes of extract used (10–20 mL). The most needed outcome of this work will be the development of value-added products from C. longa for biomedical and nanotechnology-based industries.
ISSN:0922-6168
1568-5675
DOI:10.1007/s11164-013-1040-4