A facile synthesis of (E)-3-styryl-1-phenyl cyclohepta[c]pyrazol-8(1H)-ones

A facile synthesis of some novel ( E )-3-styryl-1-phenylcyclohepta[ c ]pyrazol-8(1 H )-ones via the condensation reaction of 3-cinnamoyltropolones with phenylhydrazine is described. All the synthesized compounds were obtained in good yields of 62–69 % and their structures were characterized by IR, 1...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Research on chemical intermediates 2013-07, Vol.39 (6), p.2621-2627
Hauptverfasser: Li, Yang, Chang, Minqin, Liu, Rui, Lin, Guihai, Gao, Wentao
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:A facile synthesis of some novel ( E )-3-styryl-1-phenylcyclohepta[ c ]pyrazol-8(1 H )-ones via the condensation reaction of 3-cinnamoyltropolones with phenylhydrazine is described. All the synthesized compounds were obtained in good yields of 62–69 % and their structures were characterized by IR, 1 H NMR, MS, and elemental analysis. This procedure offers easy access to tropone-fused pyrazole derivatives in short reaction times, and the products are achieved in good yields.
ISSN:0922-6168
1568-5675
DOI:10.1007/s11164-012-0785-5