A facile synthesis of (E)-3-styryl-1-phenyl cyclohepta[c]pyrazol-8(1H)-ones
A facile synthesis of some novel ( E )-3-styryl-1-phenylcyclohepta[ c ]pyrazol-8(1 H )-ones via the condensation reaction of 3-cinnamoyltropolones with phenylhydrazine is described. All the synthesized compounds were obtained in good yields of 62–69 % and their structures were characterized by IR, 1...
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Veröffentlicht in: | Research on chemical intermediates 2013-07, Vol.39 (6), p.2621-2627 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | A facile synthesis of some novel (
E
)-3-styryl-1-phenylcyclohepta[
c
]pyrazol-8(1
H
)-ones via the condensation reaction of 3-cinnamoyltropolones with phenylhydrazine is described. All the synthesized compounds were obtained in good yields of 62–69 % and their structures were characterized by IR,
1
H NMR, MS, and elemental analysis. This procedure offers easy access to tropone-fused pyrazole derivatives in short reaction times, and the products are achieved in good yields. |
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ISSN: | 0922-6168 1568-5675 |
DOI: | 10.1007/s11164-012-0785-5 |