Preparation of Li2MoO4 using aqueous solution method and microwave dielectric properties after sintering
A novel aqueous solution method was used to prepare Li 2 MoO 4 powder, which was pressed and sintered directly into ceramic pellets without any calcination or milling stage involved. Pure Li 2 MoO 4 ceramic with the maximum bulk density of 2.898 g/cm 3 (95.63 % of the theoretical value) and excellen...
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Veröffentlicht in: | Journal of materials science. Materials in electronics 2016-05, Vol.27 (5), p.5422-5426 |
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Hauptverfasser: | , , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | A novel aqueous solution method was used to prepare Li
2
MoO
4
powder, which was pressed and sintered directly into ceramic pellets without any calcination or milling stage involved. Pure Li
2
MoO
4
ceramic with the maximum bulk density of 2.898 g/cm
3
(95.63 % of the theoretical value) and excellent microwave dielectric properties of
ɛ
r
= 5.58, Q × f = 49,328 GHz, τ
f
= −168 ppm/°C (f = 10.17 GHz) was obtained at 540 °C/2 h. The maximum Q × f value in this work is higher than that of Li
2
MoO
4
ceramic prepared by the conventional solid-state reaction method. The results show that the aqueous solution method is a simple and effective method to produce Li
2
MoO
4
ceramics. |
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ISSN: | 0957-4522 1573-482X |
DOI: | 10.1007/s10854-016-4444-2 |