Facile solvent-free synthesis and structural elucidation of styrylcyclohex-2-enone derivatives

Facile solvent-free synthesis and structural elucidation of styrylcyclohex-2-enone derivatives

A remarkably efficient procedure for the synthesis of styrylcyclohex-2-enone derivatives at room temperature is described using a mild reaction medium consisting of lithium perchlorate and N -(trimethylsilyl)diethylamine. Several compounds of this class are synthesized conveniently and rapidly. Spec...

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Veröffentlicht in:Monatshefte für Chemie 2008-08, Vol.139 (8), p.917-921
Hauptverfasser: Mojtahedi, Mohammad M., Abaee, Mohammad Saeed, Zahedi, Mohammad Mehdi, Jalali, Mohammad R., Mesbah, A. Wahid, Massa, Werner, Yaghoubi, Roholah, Forouzani, Mehdi
Format: Artikel
Sprache:eng
Schlagworte:
Analytical Chemistry
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Inorganic Chemistry
Organic Chemistry
Physical Chemistry
Theoretical and Computational Chemistry
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Zusammenfassung:A remarkably efficient procedure for the synthesis of styrylcyclohex-2-enone derivatives at room temperature is described using a mild reaction medium consisting of lithium perchlorate and N -(trimethylsilyl)diethylamine. Several compounds of this class are synthesized conveniently and rapidly. Spectroscopic and X-ray diffraction experiments confirm the proposed structures.
ISSN:0026-9247
1434-4475
DOI:10.1007/s00706-007-0847-3