Nuclear magnetic resonance for determining oil content of seeds

Twelve seed oils containing a variety of functional groups were examined with a commercial broad‐band nuclear magnetic resonance (NMR) spectrometer. Instrument response (integrator readout) was directly related to hydrogen content of the oil (r=0.999), regardless of the structures present. NMR techn...

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Veröffentlicht in:Journal of the American Oil Chemists' Society 1963-07, Vol.40 (7), p.265-268
Hauptverfasser: Conway, T. F., Earle, F. R.
Format: Artikel
Sprache:eng
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Zusammenfassung:Twelve seed oils containing a variety of functional groups were examined with a commercial broad‐band nuclear magnetic resonance (NMR) spectrometer. Instrument response (integrator readout) was directly related to hydrogen content of the oil (r=0.999), regardless of the structures present. NMR techniques were applied to the determination of oil in intact, partially dried seeds from 18 plant species containing 1.5舑53% oil having a variety of structures. The correlation between integrator readout (calculated to a uniform 25‐g sample weight) and oil content (determined by extraction with petroleum ether) is excellent (r=0.993). If the readout is further modified by a erratum for the variation in hydrogen content of the oils, the correlation becomes 0.996.
ISSN:0003-021X
1558-9331
DOI:10.1007/BF02633686