Assignment of Overlapping 1H NMR Signals in Carp Seminal Plasma by Proton-Detected 2D C,H Correlation Spectroscopy

Assignment of Overlapping 1H NMR Signals in Carp Seminal Plasma by Proton-Detected 2D C,H Correlation Spectroscopy

The 1H NMR spectrum of the perchloric acid extract of carp seminal plasma was heavily congested. It is demonstrated that proton-detected C,H chemical shift correlation spectroscopy (HSQC, HSQC-TOCSY) allows an unequivocal identification of proline, glutamate, taurine, and methionine sulfoxide, altho...

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Veröffentlicht in:Biochemical and biophysical research communications 2000-03, Vol.269 (1), p.76-80
Hauptverfasser: Kalic, Marianne, Lauterwein, Jürgen, Büsselmann, Gero, Kamp, Günter
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container_title Biochemical and biophysical research communications
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creator Kalic, Marianne
Lauterwein, Jürgen
Büsselmann, Gero
Kamp, Günter
description The 1H NMR spectrum of the perchloric acid extract of carp seminal plasma was heavily congested. It is demonstrated that proton-detected C,H chemical shift correlation spectroscopy (HSQC, HSQC-TOCSY) allows an unequivocal identification of proline, glutamate, taurine, and methionine sulfoxide, although several key proton signals were strongly overlapped.
doi_str_mv 10.1006/bbrc.2000.2250
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title Assignment of Overlapping 1H NMR Signals in Carp Seminal Plasma by Proton-Detected 2D C,H Correlation Spectroscopy
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