Synthesis, Crystal Structure and Characterization of Hexakis[2-methoxy-4-formylphenoxy]cyclotriphosphazene

Synthesis, Crystal Structure and Characterization of Hexakis[2-methoxy-4-formylphenoxy]cyclotriphosphazene

The new cyclotriphosphazene derivative N3P3(OC6H3OCH3COH)6 (1) was synthesized from hexachlorocyclotriphosphazene, N3P3Cl6, and 4‐hydroxy‐3‐methoxybenzaldehyde in acetonitrile in the presence of K2CO3. The structure of 1 was verified by means of elemental analysis, IR, 1H NMR, 13C NMR, 31P NMR spect...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Zeitschrift für anorganische und allgemeine Chemie (1950) 2008-03, Vol.634 (3), p.597-599
Hauptverfasser: Tümer, Yasemin, Bati, Hümeyra, Çalişkan, Nezihe, Yüksektepe, Çi˘dem, Büyükgüngör, Orhan
Format: Artikel
Sprache:eng
Schlagworte:
4-Hydroxy-3-methoxy-benzaldehyde
Crystal structure
Hexachlorocyclotriphosphazene
Thermal analysis
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The new cyclotriphosphazene derivative N3P3(OC6H3OCH3COH)6 (1) was synthesized from hexachlorocyclotriphosphazene, N3P3Cl6, and 4‐hydroxy‐3‐methoxybenzaldehyde in acetonitrile in the presence of K2CO3. The structure of 1 was verified by means of elemental analysis, IR, 1H NMR, 13C NMR, 31P NMR spectra, thermal analysis and X‐ray diffraction.
ISSN:0044-2313
1521-3749
DOI:10.1002/zaac.200700389