Characterization of 4,5‐Dihydro‐1 H ‐Pyrazole Derivatives by 13 C NMR Spectroscopy

The 13  C NMR resonances of 19 1‐acyl‐3‐(2‐nitro‐5‐substitutedphenyl)‐4,5‐dihydro‐1 H ‐pyrazoles, and 19 1‐acyl‐3‐(2‐amino‐5‐substituted)‐4,5‐dihydro‐1 H ‐pyrazoles, were completely assigned using the concerted application of one‐ and two‐dimensional NMR experiments (DEPT, gs‐HSQC and gs‐HMBC). Copy...

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Veröffentlicht in:Magnetic resonance in chemistry 2012-01, Vol.50 (1), p.58-61
Hauptverfasser: Carrión, M. Dora, Chayah, Mariem, Choquesillo‐Lazarte, Duane, Gallo, Miguel A., Espinosa, Antonio, Entrena, Antonio, Camacho, M. Encarnación
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Sprache:eng
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Zusammenfassung:The 13  C NMR resonances of 19 1‐acyl‐3‐(2‐nitro‐5‐substitutedphenyl)‐4,5‐dihydro‐1 H ‐pyrazoles, and 19 1‐acyl‐3‐(2‐amino‐5‐substituted)‐4,5‐dihydro‐1 H ‐pyrazoles, were completely assigned using the concerted application of one‐ and two‐dimensional NMR experiments (DEPT, gs‐HSQC and gs‐HMBC). Copyright © 2012 John Wiley & Sons, Ltd.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.2843