Pulsed field gradient one-dimensional NMR selective ROE and TOCSY experiments

Pulsed field gradient one-dimensional NMR selective ROE and TOCSY experiments

A pulsed field gradient one‐dimensional NMR selective ROE (rotating frame NOE) experiment was designed and successfully tested. The resulting spectra are of high quality and devoid of artefacts. Hence reliable quantification of very weak ROEs necessary for the three‐dimensional structure determinati...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry 1995-02, Vol.33 (2), p.156-159
Hauptverfasser: Dalvit, Claudio, Bovermann, Günter
Format: Artikel
Sprache:eng
Schlagworte:
1D-ROE
1D-TOCSY
Cyclosporin
NMR
pulsed field gradients
Selective excitation
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:A pulsed field gradient one‐dimensional NMR selective ROE (rotating frame NOE) experiment was designed and successfully tested. The resulting spectra are of high quality and devoid of artefacts. Hence reliable quantification of very weak ROEs necessary for the three‐dimensional structure determination of a molecule is now possible. A similar experiment was designed for the selective 1D TOCSY pulse sequence.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.1260330214