New pulse sequence for long-range two-dimesional heteronuclear NMR chemical shift correlation

Techniques available for long‐range heteronuclear chemical shift correlation are briefly reviewed. A new pulse sequence for long‐range heteronuclear chemical shift correlation is described. Comparison of the results obtained using the new pulse sequence with those from conventional long‐range optimi...

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Veröffentlicht in:	Magnetic resonance in chemistry 1986-12, Vol.24 (12), p.1083-1088
Hauptverfasser:	Zektzer, Andrew S., Quast, Michael J., Linz, Gary S., Martin, Gary E., McKenney, J. Dew, Johnston Jr, Milton D., Castle, Raymond N.
Format:	Artikel
Sprache:	eng
Schlagworte:	Heteronuclear proton-carbon chemical shift correlation Long-range optimization Long-range proton-carbon chemical shift correlation Two-dimensional NMR
Online-Zugang:	Volltext
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Zusammenfassung:	Techniques available for long‐range heteronuclear chemical shift correlation are briefly reviewed. A new pulse sequence for long‐range heteronuclear chemical shift correlation is described. Comparison of the results obtained using the new pulse sequence with those from conventional long‐range optimized heteronuclear chemical shift correlation is presented. Total Assignments of the 1H and 13C NMR spectra of 1‐benzothieno[2,3‐çlquinoline], the model compound used for the study, are reported.
ISSN:	0749-1581 1097-458X
DOI:	10.1002/mrc.1260241213